By Michael D. Cole
Offering new advancements in sampling and drug profiling, this publication additionally offers sensible details on how one can perform research, what the consequences suggest and the way they are often used as courtroom proof and for medicinal drugs intelligence purposes.
* comprises case-studies with complete info and spectra, supporting readers to spot substances
* Accessibly geared up through category of compound
* comprises an up to date record of the most recent medicinal drugs
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Extra resources for Analysis of Controlled Substances
49, 205–213 (1991). 9. , Gueniat, O. and Cole, M. D. ‘Identiﬁcation and quantiﬁcation of amphetamine and analogues by capillary zone electrophoresis’, Sci. Justice, 37, 113–119 (1997). 10. Lurie, I. , Bethea, M. , McKibben, T. , Hays, P. , Garcia, A. D. , ‘Use of dynamically coated capillaries for the routine analysis of methamphetamine, amphetamine, MDA, MDMA, MDEA and cocaine using capillary electrophoresis’, J. , 46, 1025–1032 (2001). 11. White, P. , personal communication. 12. Jonson, C. S.
To be aware of the chemical and ﬂuorescence testing procedures for LSD. • To understand the principles of TLC analysis of LSD. • To be aware of the conﬁrmatory techniques available for the analysis of LSD. 1 Introduction While a large number of drugs are known which are of plant origin, or have plant products as starting materials for the synthesis of the drugs, there are, equally, a number of drugs of fungal origin. e. well known, and it is on this drug that this chapter focuses. Interestingly, the drug is an indole alkaloid which presents special difﬁculties and opportunities in terms of drugs analysis.
The three principle routes of synthesis are the Leuckart synthesis, the reductive amination of benzyl methyl ketone (BMK) and the nitrostyrene route. It is not the intention here to provide the ‘recipes’ for these syntheses – they may be readily obtained from the refereed scientiﬁc literature and the Internet, although brief outlines are given below. What is intended is to illustrate the different types of impurities which can provide signatures when different routes are used, to discuss the extraction and analysis of the impurities, and the interpretation of the data following such analyses.